Regulation of Fuels and Fuel Additives: Standards for Deposit Control Gasoline Additives

Federal RegisterDec 28, 1994

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Text

40 CFR Part 60

40 CFR Part 80

[AMS-FRL-5128-9]

Regulation of Fuels and Fuel Additives: Standards for Deposit

Control Gasoline Additives

AGENCY: Environmental Protection Agency (EPA).

ACTION: Proposed rule; reopening of comment period.

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SUMMARY: On December 6, 1993, EPA published a Notice of Proposed

Rulemaking (NPRM) to require the use of deposit control (detergent)

additives in all gasoline used in the United States. The NPRM contained

a proposed interim program which would take effect beginning January 1,

1995, as well as a proposed performance-based detergent additive

certification program to be implemented at a later date. The interim

program was finalized on October 14, 1994. The detergent certification

program is expected to be finalized by June 30, 1995, and to take

effect a year later.

As proposed, the detergent certification program was concerned

specifically with the control of port fuel injector deposits (PFID) and

intake valve deposits (IVD). While also acknowledging the potential

importance of combustion chamber deposits (CCD), EPA did not propose

any requirements for CCD control because of uncertainty regarding the

scope of the problem and the current lack of suitable performance test

procedures and standards. Subsequently, some commenters expressed

concern that a federal requirement for PFID and IVD control might

encourage detergent overuse, which could potentially exacerbate CCD

concerns. These commenters suggested that, as a temporary measure,

until CCD performance tests become available, EPA should cap detergent

use by implementing standards to limit the level of unwashed gums in

additized gasoline. However, other commenters disagreed with this

suggestion. This document discusses the CCD issue and requests comments

on alternative approaches for addressing it. Additional comment is also

sought in regard to selected issues related to the proposed detergent

certification program and the enforcement provisions of the detergents

program.

DATES: Written comments on the specific issues discussed in this

document will be accepted until January 27, 1995. EPA is not soliciting

new comments on aspects of the original proposed rule that are not

specifically addressed in this document.

ADDRESSES: Comments on this notice should be submitted in duplicate to:

EPA Air Docket Section (LE-131); Attention: Public Docket No. A-91-77;

Room M-1500, 401 M Street S.W., Washington, DC 20460. (Phone 202-260-

7548; FAX 202-260-4000). This docket also contains all other materials

relevant to this rulemaking. The docket is open for public inspection

from 8:00 a.m. until 4:00 p.m., except on government holidays. As

provided in 40 CFR part 2, a reasonable fee may be charged for copying

docket materials.

Electronic copies of this and other documents related to this

rulemaking are available through the Office of Air Quality Planning and

Standards (OAQPS) Technology Transfer Network Bulletin Board System

(TTNBBS). Details on how to access this bulletin board are included in

Section VII of this notice.

FOR FURTHER INFORMATION CONTACT: For general information and

information related to technical issues contact: Mr. Jeffrey A. Herzog,

U.S. EPA (RDSD-12), Regulation Development and Support Division, 2565

Plymouth Road, Ann Arbor, MI 48105; Telephone: (313) 668-4227, Fax:

(313) 741-7816. For information on enforcement related issues contact:

Judith Lubow, U.S. EPA, Office of Enforcement and Compliance Assurance,

Western Field Office, 12345 West Alameda Parkway, Suite 300, Lakewood,

CO 80228; Telephone: (303) 969-6483, FAX: (303) 969-6490.

SUPPLEMENTAL INFORMATION:

I. Introduction

Section 211(l) of the Clean Air Act (CAA) specifies that, beginning

January 1, 1995, all gasoline shall contain additives to prevent the

accumulation of deposits in engines or fuel supply systems. Such

deposits can have adverse effects on the emissions of a vehicle as well

as its fuel economy and driveability. As part of the CAA mandate, EPA

was tasked with the promulgation of rules establishing specifications

for such additives.

In response to these statutory requirements, on December 6, 1993,

(59 FR 64213) EPA published a Notice of Proposed Rulemaking (NPRM)

requiring that gasolines contain detergents to control port fuel

injector deposits (PFID) and intake valve deposits (IVD). The rule was

proposed to be implemented in two phases. The first phase was an

interim program focused on registration and record-keeping requirements

which would apply for the first year. The second phase, to apply

thereafter, was a certification program requiring detergents to be

evaluated in a matrix of test fuels using national consensus test

procedures and prescribed standards for IVD and PFID control.

The detergents rule is being finalized in two parts. The interim

program was promulgated October 14, 1994, and appeared in the Federal

Register on November 1, 1994 (59 FR 54678). Promulgation of the full

detergent certification program is expected to occur by June 30, 1995.

This second phase of the rule was delayed for two reasons. First, the

national consensus procedure EPA proposed for use in testing PFID

control was not finalized by the American Society for Testing and

Materials (ASTM) in time to be incorporated into the rule. Since an

interim program had already been proposed for 1995, EPA saw little

value in abandoning reliance on the ASTM procedure solely for the sake

of promulgating the entire rule at once. Second, issues were raised in

the comments regarding the possible impact of IVD and PFID control

requirements on combustion chamber deposits (CCD).

While the NPRM also contained a substantial discussion on CCD, it

did not propose specific CCD control measures due to a lack of national

consensus test procedures and performance standards as well as

uncertainty as to the scope of the CCD problem. Given the need for a

slight delay in the final rulemaking schedule to allow completion of

the test procedure development, EPA believed it was important to

further evaluate the CCD issue prior to finalization of the

certification program.

As part of that evaluation effort, this notice seeks public comment

on concerns raised by auto industry commenters that the gum levels in

gasoline will increase as a result of the use of IVD and PFID detergent

additives and that these gums will increase CCD. This could have an

adverse effect on emissions and vehicle driveability. Additional

comment is also sought on several points raised in the comments

regarding the proposed implementation and enforcement schemes under the

detergent certification program. Each of these areas is discussed

below.

II. Combustion Chamber Deposit Control

A. Background

CCDs are composed of fuel and other material which enter the

combustion chamber, are not fully burned, and are deposited in various

portions of the engine's combustion chamber rather than leaving the

chamber with other exhaust products. The formation of CCD is governed

by the combustion process, combustion temperatures, and the design of

the combustion chamber itself. Other factors influencing CCD formation

include fuel and oil composition, engine design/technology and

operating conditions (e.g., speed, load, coolant temperature), engine

oil consumption, and fuel/oil additive usage. The technical literature

indicates that CCD potentially have three effects on engine operations:

an adverse effect on emission rates, an increase in engine octane

requirements, and an impact on fuel economy. Additional background

information on CCD is provided in the NPRM as well as a memorandum to

the docket entitled, ``Summary Discussion of Combustion Chamber

Deposits'' (Docket Item IV-B-04).

Based on the incomplete information available in the literature and

the lack of available consensus test procedures or standards, EPA did

not propose a requirement for CCD control related to emissions or

octane requirement increase (ORI) effects. EPA received comments both

supporting and opposing this position.

Vehicle manufacturers expressed concern that the proposed rule,

which contained IVD/PFID performance standards but no requirements to

control CCD, may have an adverse impact on vehicle performance. They

stated that the use of excessive quantities of some types of detergent

additives, which provide an acceptable level of IVD/PFID control, tend

to incrementally contribute to CCD. They further held that EPA's rule,

by requiring a consistent level of IVD/PFID control additives in all

gasoline, may exacerbate this incremental additive contribution to CCD,

since there would be at least a slight incentive to over- additize fuel

to assure compliance. An adverse impact on vehicle NOx and HC emissions

performance and durability would result.

Vehicle manufacturers also stated that CCD can cause ORI, and that

higher engine octane demand might limit future attempts to achieve fuel

economy improvements through the design of engines with higher

compression ratios. Concerns regarding the potential impact of CCD on

vehicle driveability and durability centered around reports that

detergent additive overuse could result in valve sticking and

combustion chamber deposit interference (CCDI). These commenters stated

that CCDI results from the accumulation of CCD on the top of the piston

and combustion chamber, which causes mechanical interference during

engine operation.

Vehicle manufacturers urged EPA to investigate the potential

adverse impact of some IVD/PFID additives on CCD as soon as possible,

with the ultimate goal of a standardized CCD control test. As an

interim measure, until such a performance test is available, several

commenters urged EPA to, in effect, adopt a cap on additive

concentration, by setting a maximum unwashed gum level in additized

gasoline as measured by ASTM test D381. Two vehicle manufacturers

recommended an unwashed gum standard of 20 mg/100 ml, based on the

allowable limit for Japanese gasoline. They stated that CCD problems

are not present in vehicles in Japan and this may be due in large part

to the unwashed gum standard of 20 mg/100 ml. The American Automobile

Manufacturers Association (AAMA) recommended an unwashed gum limit of

70 mg/100 ml, and stated that this value would act as a cap and not

create a large burden since it exceeds the levels found in most

gasolines today. These commenters supported their position by stating

that a relationship exists between the increased use of IVD detergent

additives, an increase in unwashed gum levels in gasoline, and an

increased incidence of CCD-related customer complaints.

One vehicle manufacturer recommended that, as a condition for

detergent certification, data should be required demonstrating that the

additive does not increase CCD relative to base gasoline. This

commenter further stated that it would be appropriate in the interim to

allow each additive manufacturer to use its own CCD control test

methods. The commenter stated that, because these test procedures would

be expected to vary from manufacturer to manufacturer, this approach

was recommended only as an interim solution until a standardized CCD

performance test and standard is developed.

In contrast to the vehicle manufacturers, the petroleum and

additive industries contended that regulatory control of CCD was not

appropriate at this time because of a lack of data on the effects of

CCD and the lack of an adequate performance test and standard. They

stated that data suggesting a link between additive use and increased

CCD with associated increased emissions and ORI is too sparse to reach

sound conclusions. These commenters also stated that engine

manufacturing tolerances may play a greater role than fuel properties

in determining the onset and occurrence of CCDI. Commenters from the

petroleum industry stated that, while negative impacts from

overtreatment exist, including valve sticking, these occurrences have

been very rare and usually result from an accidental overtreatment. In

summary, API stated that there is no immediate, growing CCD-related

problem in the field, and EPA's planned IVD/PFID control requirements

are not likely to cause one. They stated that regulatory control of CCD

should not be attempted until the Coordinating Research Council (CRC)

has had an opportunity to investigate potential adverse effects of CCD

and to gain an understanding of all of the factors which can affect

CCD, including hardware, lubricant, fuel and additive effects.

Commenters from the petroleum industry all agreed that, even if the

need to control CCD were demonstrated, setting a cap on the unwashed

gum level in additized gasoline would not be an appropriate control

measure. They argued that the data offered to support a correlation

between unwashed gum levels and CCD formation is unreliable.

Furthermore, they claimed that the unwashed gum test is highly

unrepeatable and cannot differentiate different sources of the gum

content in the gasoline. They also noted that, since many current IVD/

PFID detergents have varying levels of dispersant and carrier oils

(some having no carrier oil), the unwashed gum level in gasoline can be

highly misleading as a measure of the amount of additive present.

Given the disparity in these positions, EPA requested additional

input from the affected industries. Additional comment was received

from AAMA, API, Shell Development Company, and the Chemical

Manufacturer's Association (CMA)\1\ Two technical papers were also

published in this time frame that presented additional useful data on

CCD related issues.\2\

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\1\See the memorandum to the docket entitled ``Summary of

Additional Comments on Combustion Chamber Deposits'', Docket Item

IV-E-35. Discussion of additional comments on CCD is also contained

in the following docket items: IV-E-12, IV-E-27, IV-E-29, IV-E-33,

IV-E-36, IV-G-37, and IV-E-38.

\2\``Effects of Gasoline and Gasoline Detergents on Combustion

Chamber Deposit Formation'', Yasunori Takei et. al., SAE Technical

Paper Series No. 941893. ``Effects of Fuel and Additives on

Combustion Chamber Deposits,'' Mitchell Jackson and Sara Pocinki,

SAE Technical Paper Series No. 941890.

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B. Considerations for Determining a Course of Action

EPA is considering the implementation of a CCD control measure at

this time in view of auto industry concerns that, absent such a

measure, EPA's planned detergent certification program might contribute

to CCD-related vehicle performance problems. Any CCD control measure

which EPA might require must be based on EPA's belief that such a

measure would prevent a future CCD problem or solve one which now

exists. In addition, it would have to be practical to implement and be

founded on a sound understanding of its impacts. If a control program

is found to be needed, it would preferably be based on a national

consensus test procedure and performance standard. Because several

years may be required to develop such a test procedure and standard,

however, a cap on unwashed gums has been suggested as a surrogate CCD

control strategy. Thus, to determine whether it is appropriate for EPA

to implement an unwashed gum standard for additized gasoline as an

interim measure to control the potential additive contribution to CCD,

EPA must assess the following questions:

1. To what extent do some or all IVD/PFID detergents contribute to

unwashed gum levels in gasoline? Which, if any, classes/types of

additives are of concern? Under what conditions and how substantial is

this contribution?

2. To what extent do gums added to gasoline as part of the

detergent additive package correlate or contribute to CCD formation?

3. To what extent is there now a CCD problem associated with the

voluntary use of IVD/PFID detergents? Will mandatory use of these

detergents exacerbate the potential concerns?

4. To what extent do CCD cause vehicle emission and performance

problems?

The information found in the literature and presented by the

industry either in their written comments or in response to EPA follow-

up is helpful in answering these questions. However, more information

is needed. These points are discussed below, followed by a discussion

of various alternatives that EPA could adopt regarding CCD control. EPA

encourages public comment that would help to further the understanding

of these issues.

1. Additive Contribution to Gasoline Unwashed Gum Levels

The data summarized in the previous section indicate a trend toward

increased unwashed gum levels with increased detergent additive use and

concentration. Public comment is sought on the unwashed gum levels in

additized gasoline for both the various classes/types of detergent

additives and individual detergent products. Information is also sought

on the relative contribution of various detergent additive package

components to unwashed gums. In addition, EPA is also interested in

more detail and public comment on claims that some detergents with

superior CCD control performance cause relatively high unwashed gum

levels in gasoline.

2. Gum/Additive Package Contribution to CCDs

The information available seems to support the view that some

detergent additives contribute to CCD more than others. However, the

significance of this contribution relative to the potential adverse

impacts of CCD remains unclear. It is also not completely clear what

fraction of the additive types currently used contribute to CCD. This

may be a significant concern if a CCD control measure were considered

that would preclude the use of a significant fraction of the detergents

currently being used. EPA understands that PIBA type detergent

additives that use a mineral-based carrier oil predominate in the

market. EPA requests comment on several points. First, more data is

requested on the relationship between gums, the additive packages, and

CCD. Second, EPA is interested in information on which classes/types of

additives contribute to this concern more than others and market share

and cost information on each type. Third, EPA requests comment on

whether the use of a synthetic-based carrier oil rather than a mineral-

based carrier oil in PIBA detergents would decrease the gum levels and

improve the CCD impacts of these additives and the economic impacts

which might result from such a change.

3. Prevalence of CCD-Related Problems Due to Detergent Use and the

Effect of IVD Control Requirements on CCD

More information is needed to quantify the scope of the current CCD

problem as it relates to detergent additives. Additional information is

needed on the fraction of vehicles with CCD-related performance

problems as well as estimates of how the problem could grow with

federal detergent requirements. Some public comment presented the

viewpoint that the planned IVD/PFID control requirements would not

result in over-additization because the primary result would be the use

of deposit control additives by all fuel marketers at levels that are

currently achieved in the majority of gasoline sold within the U.S.

However, this comment neglects concerns about possible over-

additization to assure compliance during field enforcement as well as

for marketing/advertising purposes. EPA encourages additional comment

on this issue.

4. Potential CCD-Related Vehicle Emissions and Performance Impacts

A review of the available data on the potential impact of CCD on

exhaust emissions is suggestive of a potentially significant impact.

However, in addition to the prevalence issue discussed above, comment

is requested in a number of areas relative to this point. First,

comment is requested regarding the role of vehicle technology on the

sensitivity to CCD. Second, more information is requested regarding a

potential for threshold effect(s). Is there a level below which no CCD

effect occurs for emissions, CCDI, ORI, or fuel economy? If thresholds

exist, do they vary for the different impacts? In what relative order?

Is there a CCD level above which the level of CCD no longer exacerbates

the impact? If such thresholds exist, any potential control measure

would ideally need to result in the reduction of CCD beyond this

threshold to ensure any meaningful emissions benefit. Since there may

be a threshold effect for the impact of CCD on fuel economy, the

relationship of this threshold to the possible threshold for exhaust

emissions and other impacts would also need to be considered in

evaluating the overall impact of a CCD control measure. Third, data is

needed relating these threshold effects to the amount of detergent

additive used. EPA welcomes the submission of any data which might help

to clarify these issues.

The data on CCDI is also not conclusive as to whether this problem

is related to fuel quality or vehicle manufacturing problems. EPA

encourages the submission of additional data to further evaluate this

issue. Of particular value would be data illustrating the extent to

which out-of-tolerance engine manufacture may play a role.

The commenters agreed that problems with intake valve sticking

sometimes result from detergent additive overtreatment. However,

opinions differed as to the extent of these problems and their

relevance to the possible necessity of a standard to limit detergent

additive concentration. The data currently available is limited and EPA

encourages the submission of additional data to help determine the

prevalence of this problem. The data on the potential impact on vehicle

performance associated with oil viscosity increase (OVI) from the use

of detergent additives is likewise very limited and more data is

requested in this area.

C. Alternative Actions Which EPA Could Adopt

Based on the information already available and any additional

information received in response to this notice, several options will

be considered. Each of these is discussed below.

1. Option 1: Follow Approach Proposed in NPRM

The first approach to the CCD issue that EPA is considering is to

follow the basic strategy outlined in the NPRM. Under this option, EPA

would defer action on CCD pending the gathering of more data, while

encouraging responsible actions by industry to develop an industry

consensus test procedure and standard. The CRC CCD panel may be in the

best position to lead development of national consensus test procedures

and standards for CCDs. However, EPA is aware of the disagreement among

members of the industry regarding the current direction of the CRC CCD

panel's work. Thus, there is considerable uncertainty as to the

viability of this option. Members of the CRC's panel from the

automobile industry have expressed reservations about whether the

investigative work of the CRC CCD panel will proceed rapidly enough to

address their concerns regarding the potential impact of CCD on vehicle

driveability and on in-use emissions. EPA requests comment on whether

it is appropriate to allow industry to evaluate CCD related issues

further prior to initiating any potential regulatory action regarding

CCD control, or if more immediate intervention on the part of the

Agency is necessary.

2. Option 2: Consideration of a CCD Performance Standard

As discussed above, the Agency concluded in the proposal that the

lack of adequate data relating CCD to emissions, ORI, or other engine

performance indicators, as well as the lack of a suitable test

procedure, precluded the Agency from proposing a CCD-related detergent

additive performance standard at that time. However, the Agency stated

that it may, at a later time, propose test procedures and performance

standards for the control of CCD (among other deposit-related

phenomena).

In light of recent events (e.g., receipt by EPA of written and

verbal comments concerning issues not considered previously), the

Agency is again considering the issue of whether or not EPA should

pursue such a combustion chamber deposit control performance standard

at this time. A discussion of specific issues related to the

development of a CCD performance standard is provided in a memorandum

to the docket entitled, ``Consideration of a Combustion Chamber Deposit

Control Performance Standard'' (Docket Item IV-B-05).

3. Option 3: Require Data Submission on Unwashed Gums

As an intermediate measure, EPA could require that data on the

unwashed gum levels of additized gasoline be submitted as part of

detergent certification. Under this option, the detergent certifier

would be required to measure the unwashed gum levels in their

certification test fuel using the ASTM D-381 test procedures (see next

section). The only requirement would be that these measurements be

reported to EPA. Using these data, EPA could assess the difference in

unwashed gum levels relative to the chemistry of the detergent additive

package to evaluate whether a correlation exists. This information

would also be useful in determining what fraction of gasoline is

treated using additives that cause high unwashed gum levels for the

purposes of evaluating the potential effect on industry of implementing

an unwashed gum standard or CCD control program in the future.

This option would also be beneficial in that it would encourage

continued industry focus on CCD-related issues and may encourage the

use of additives with better CCD control performance or less of an

impact on unwashed gum levels. An unwashed gum reporting requirement

would have little economic impact on industry, since the testing would

be conducted concurrent with detergent certification testing, would not

require a separate submittal to the Agency, and would be of minimal

cost. EPA requests comments on the potential benefits and usefulness of

this option in responding to current CCD concerns, and on any

additional data that EPA should require to be submitted during

detergent certification to help evaluate whether a CCD control measure

based on an unwashed gum specification is appropriate.

4. Option 4: Implement an Unwashed Gum Standard

As a measure to address concerns that detergent over-additization

would contribute to CCDs, EPA requests comment on whether it would be

appropriate to implement a limit on the unwashed gum level in additized

gasoline as part of the requirements for detergent certification. As

previously discussed, questions remain regarding the need for a full

regulatory program to control CCD effects, and the potential associated

impacts on emissions, fuel economy and vehicle driveability. While some

public comments suggest that limiting the additive contribution to

unwashed gums would not necessarily always result in a reduction in

CCD, it is possible that an intermediate measure such as this would

address the most significant concerns raised by the auto industry

commenters without levying large direct compliance costs on the fuel

and detergent additive industries. As perceived by the regulated

industry the benefits may be very small, but, as discussed below, costs

would also be very small. On the other hand, this requirement could

make detergent packages with higher gum levels less attractive and

could act as a disincentive for research on detergent additive packages

with high gum levels. If an unwashed gum standard is established, EPA

asks comment on whether such a standard should only be implemented for

an interim period, assuming a CCD test procedure/ standard is

established by regulation.

a. Unwashed Gum Test Procedure. If an unwashed gum standard is

adopted, it would likely need to be implemented by requiring testing of

unwashed gum levels in detergent-additized gasoline using the ASTM D381

procedure or a derivation of this procedure. Concerns have been raised

about the repeatability and reproducibility reported for this procedure

in the ASTM D381 document, and EPA believes it would be useful to

further explore the reasons for the reproducibility and repeatability

performance cited in the procedure. In discussions with industry

experts regarding the ASTM D381 procedure, one member of the panel

which originally developed the procedure suggested the possibility that

greater precision might be expected in measuring the unwashed gum

levels of modern gasoline. The repeatability/reproducibility data in

the ASTM procedure is based on gasolines of the 1960s and 1970s.\3\ EPA

requests comment on the extent to which gasoline composition can effect

the precision that can be achieved in the ASTM test.

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\3\Memorandum to the docket entitled, ``Phone Call with Leo

Stavinola of Southwest Research Institute (SwRI), Regarding the

Applicability of the Unwashed Gum Test to Modern Gasoline'', Docket

Item IV-E-33.

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EPA's analysis of 1993-94 unwashed gum data collected under ASTM's

Interlaboratory Crosscheck Program suggests that the current

reproducibility of the procedure may be somewhat better than that

reported in the D381 document.\4\ However, the limited range of

unwashed gum values represented in the test samples prevents an

accurate assessment of test variability over the range of unwashed gum

values likely to be encountered in use.

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\4\Report to EPA from George Hoffman, CSC, entitled ``Sample

Sizes for Unwashed Gums Measurements''.

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Not all laboratories using the D381 unwashed gum procedure

encounter the variability discussed in the ASTM document. EPA contacted

Southwest Research Institute (SwRI) to further evaluate the suitability

of the unwashed gum test from the standpoint of repeatability and

reproducibility.\5\ SwRI stated that the unwashed gum test is used

routinely by their laboratory to determine whether or not gasoline had

been detergent additized. In addition, SwRI related that not only was

this test a useful predictor of additive presence, but it could also

distinguish additive concentration fairly well. SwRI stated that, in

their considerable experience in performing the unwashed gums test,

they have achieved significantly better repeatability than that

reported in the ASTM procedure. For example, at an unwashed gum level

of 60 mg/100 ml, they commonly achieve repeatability of results within

5 mg/100 ml, as compared to the 25 mg/100 ml

reported in the ASTM procedure. A round robin program conducted by AAMA

using three fuels and four labs also indicated good reproducibility

(coefficients of variation of 6 percent, 12 percent, and 2 percent) for

the three fuels tested. (See memo in public docket at IV-G-39).

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\5\Memorandum to the docket entitled ``Phone Call with Karen

Kohl of Southwest Research Institute (SwRI) Regarding the Unwashed

Gums Test,'' Docket Item IV-E-32.

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SwRI stated that they are aware of several potential problems that

may partially account for the poor reproducibility reported by ASTM.

SwRI related that the temperature of the evaporation bath and the flow

of air to the airjet apparatus must be carefully controlled to limit

the variability in results. SwRI also related that another potential

problem which can introduce variability in test results is

contamination of the oil from the supply pumps. If the repeatability

reported by SwRI and the reproducibility achieved in the AAMA study

could also be achieved at other laboratories, it might be possible to

achieve adequate test precision while minimizing the required number of

repeat tests.

EPA requests comment on ways in which the ASTM D381 procedure could

be modified to limit test variability. In particular, EPA requests

comment on whether additional specifications are required regarding

control of the evaporation bath temperature, flow of air to the air jet

apparatus, and prevention of oil contamination of the fuel sample from

the supply pumps. Specifically, EPA is considering tighter

specifications on several elements of the test including the air jet

apparatus to 600mL/s 30 mL/s, the steam jet apparatus to

1000 mL/s 50 mL/s, and the evaporation bath well

temperature to 155 deg.C 2 deg.C. Use of a temperature

measuring approach other than a thermometer (e.g., thermocouple with

digital readout) is also being considered. Other similar modifications

to test specifications will also be considered to the degree that they

would reduce variability. The submission of test data from the ASTM

D381 procedure would also be useful in assisting further evaluation

evaluating test repeatability and reproducibility.

b. Unwashed Gum Limit. If an unwashed gum standard for additized

gasoline is adopted, it must be carefully selected based on the

consideration of several factors. First, the available data suggests

that the contribution to unwashed gums from sources other than

detergent additives is generally under 10 mg/100 ml per the ASTM test.

This consideration is important because the focus of an unwashed gum

standard must be on the additive contribution to gums. EPA believes

that it may be reasonable to assume that the base fuel contribution to

gasoline unwashed gum levels does not exceed 10 mg/100 ml. EPA requests

data to further evaluate whether this assumption is appropriate.

Second, the choice of an unwashed gum cap should be based on an

understanding that such a cap would result in an appropriate level of

CCD control. This involves consideration of the possible threshold

effects of CCD-related emissions, fuel economy, and vehicle

driveability impacts. EPA requests comments on what would be an

appropriate unwashed gum cap given these considerations.

There were two separate suggestions in the public comment regarding

the choice of an appropriate unwashed gum cap. The first suggestion was

to adopt the unwashed gum cap already in place for Japanese gasoline of

20 mg/100 ml.\6\ This suggestion was based on the premise that the 20

mg/100 ml cap has been in force for Japanese gasoline for some time,

that industry has been able to comply with this cap while meeting other

deposit control performance needs, and that the presence of such a cap

might be credited for the absence of CCD-related problems in Japan. EPA

is concerned about setting a potential standard at this level, because

it would prevent the use of many current IVD/PFID detergents. Assuming

absolute precision in unwashed gum measurement, a 20 mg cap would limit

the additive contribution to unwashed gums to about 10 mg. The

available data indicates that this is significantly less than the

contribution to unwashed gums for IVD/PFID detergents currently used in

the U.S. which typically appears to be between 20 and 60 mg/100 ml and

can be considerably higher.\7\ EPA's review of AAMA gasoline survey

data reveals that less than 40 percent of U.S. gasoline samples tested

had an unwashed gum level below 20 mg/100 ml.\8\ One explanation for

the apparent large difference in unwashed gum levels in Japanese and

U.S. gasolines might be that Japanese gasoline tends to require less

detergent for adequate IVD control. EPA requests comment that would

help explain the difference between the unwashed gum levels in Japanese

and U.S. gasoline.

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\6\Written comments on the NPRM from Mazda Motor Corporation,

Docket Item IV-G-17, and from Toyota Motors Inc., Docket Item IV-G-

25.

\7\Letter to Glenn Passavant, Office of Mobile Sources, from

James Williams, American Petroleum Institute, Docket Item IV-G-36.

\8\AAMA unleaded gasoline survey data, 1991-1993, California

gasoline excluded.

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AAMA suggested a significantly higher unwashed gum cap than that

observed in Japan. AAMA contended that their suggested cap of 70 mg/100

ml took into account the base gasoline contribution to gums and the

variability in the ASTM test procedure, and would allow the use of

detergents capable of IVD, PFID and CCD control. They further stated

that compliance with this cap could be achieved using current additive

technology that results in unwashed gum levels of 35 to 40 mg/100 ml.

AAMA's suggestion is based on the premise that an appropriate level of

control of the detergent additive contribution to CCD can be achieved

by preventing the use of the highest concentrations of detergent

additives and unnecessary over-additization. EPA's review of AAMA

gasoline survey data reveals that more than 90 percent of U.S. gasoline

samples analyzed had unwashed gum levels below 70 mg/100 ml. A review

of the same data also showed that approximately 35 percent of U.S.

gasoline had unwashed gum levels in excess of 40 mg/100 ml. Thus,

depending on the precision of the unwashed gum test, a 70 mg/100 ml

unwashed gum cap could result in disqualification for use of detergent

packages/concentrations used in approximately 10 to 35 percent of

gasoline in the U.S.

EPA requests comment on the suitability of an unwashed gum cap of

70 mg/100 ml. In particular, EPA requests comment on the potential

benefit of implementing such a standard, and the ability of industry to

meet IVD/PFID deposit control requirements with additives that comply

with a 70 mg/100 ml unwashed gum standard.

Given concerns expressed by some commenters about variability, EPA

proposes that certification or data submission requirements be based on

the average of five unwashed gum tests (ASTM D381). With regard to an

unwashed gum standard, EPA asks for comment on the minimum number of

unwashed gums tests which should be specified to demonstrate compliance

and, as an option to industry, the maximum number which could be

allowed.

c. Incorporation of Unwashed Gum Standard Into the Detergent

Certification Program. If EPA adopts an unwashed gum standard or

requires submission of unwashed gum levels, the primary compliance

focus would be placed on unwashed gum testing of the properly additized

test fuel(s) used during detergent certification. One option would be

to require the measurement of the unwashed gum level of a test fuel

blended with the minimum treatment rate of the detergent package as

determined by certification testing for IVD/PFID control. To limit

variability in the base fuel contribution to unwashed gums, the test

fuel would be required to comply with other specifications regarding

gasoline composition (i.e., aromatic, olefin, T-90 and oxygenate

content) prescribed for detergent certification testing. For the

detergent additive to be certified, the unwashed gum level in this test

(or the average for a series of tests) would need to be below the

unwashed gum standard.

One of the major issues raised by the auto industry commenters was

concern that over-additization could lead to increased gum levels and

CCD-related problems. While there may be no economic incentive to over-

additize, it is likely to occur. It may occur accidentally, some fuel

manufacturers may choose to slightly over-additize to ensure compliance

with the volume accounting reconciliation requirements of EPA's

enforcement program, or it may occur for other reasons such as

advertising. One way to accommodate these possibilities and yet also

address the concerns of auto makers is to set the concentration of the

additive in the test fuel during testing for unwashed gums at a level

higher than the certified treat rate. For example, requiring

certification to the unwashed gum standard (or testing of unwashed gums

under Option 3) at a level of 110 percent of the certified treat rate

would allow the assessment of the impact of a slight over-additization

without creating an unreasonable obstacle to compliance. This would

also allow for some variation in the unwashed gum level of the

unadditized gasoline. Yet another approach with a similar effect would

be to reduce the proposed standard by 10 percent. That is, instead of

20 mg/100 ml or 70 mg/100 ml, the standard would be set at 18 mg/100 ml

or 63 mg/100 ml with testing conducted at the certified treat rate.

The detergent registration and certification programs require that

each gasoline contain detergent in an amount at least equivalent to the

minimum certified treat rate. No maximum limit is anticipated. While

testing at 110 percent of the minimum certified treat rate would

address slight over-additization when the minimum treat rate is the

actual target concentration, it will not be representative for fuels

additized at even higher rates. EPA, therefore, asks comment on an

option which would require those fuel manufacturers who add detergent

at greater than 110 percent of the minimum treat rate to pass the

unwashed gum standard using fuel treated at the rate actually being

used.

As an ancillary enforcement tool, EPA might also require the

submission of test data on the unwashed gum levels of in-use fuels from

detergent additive blenders. In-use testing of unwashed gum levels

might also be conducted by EPA. EPA does not anticipate that such in-

use testing would be conducted routinely, but rather that it would be

used in cases where there was a suspicion of violation, or would be

conducted randomly to encourage compliance. Penalties for noncompliance

with an unwashed gum standard would be similar to those for

noncompliance with minimum concentration requirements. EPA requests

comments on the potential certification and enforcement requirements

described above as well as input on other options.

d. Costs and Benefits. The potential economic impacts of

implementing an unwashed gum standard or data submission requirement

vary with the provisions of the potential program, but in general would

be similar. First, EPA needs to further evaluate the number of unwashed

gum tests that would be required for each detergent certification. If a

single unwashed gum test was performed during certification testing,

the additional cost for each certification would be approximately $100

for a total cost to industry of approximately $40,000 for the

approximately 400 detergents certified in the first year of the

program. (This assumes that these tests are not already conducted for

other reasons. If multiple tests are used to reduce variability

concerns raised in association with the ASTM D381 test, the total cost

would be somewhat higher. If, for example, five tests were conducted as

proposed above, the total cost for all detergents would be $200,000 in

the first year. Recurring annual costs would vary between $6,000 and

$30,000 assuming 15 percent new certifications per year.

While it may be difficult to quantify the emission benefits, it is

possible to estimate whether such a program could be cost effective.

One approach would be to calculate the amount of emissions that would

need to be prevented by an unwashed gum standard for the control

measure to be cost-effective. If the costs were low, the amount of

emissions that would need to be prevented could be relatively small and

yet the program could still be quite cost effective. Using the first

year cost of $200,000 discussed above, only 200 tons of HC/NOx emission

reductions would be required to achieve a nominal cost effectiveness of

$1,000 per ton. Given the large number of miles travelled per year by

gasoline-fueled vehicles, only a tiny fraction of the fleet would have

to get a tiny benefit for this level of benefits to be achieved. For

example, less than a hundredth of one percent of vehicles would have to

achieve a 0.01 g/mi benefit in order to achieve this benefit. This

level of benefits and more appears quite conceivable. The potential

negative impact of fuel economy that may accompany a reduction in CCDs

complicates consideration of the potential economic impact of the

program, as do potential adverse impacts on companies manufacturing

detergent additives with high unwashed gum levels. EPA requests comment

on the approach to determine the cost- effectiveness of CCD control

outlined above and on a method by which any potential negative impact

on fuel economy might be accounted for. EPA also asks comment on

whether it is possible to reduce emissions or prevent emission problems

without adversely affecting fuel economy. It should be noted that

section 211(l) of the CAA does not require EPA to justify deposit

control measures on a cost-effectiveness basis. However, EPA will give

the costs and benefits of any potential CCD control measure due

consideration.

5. Other Options

a. Use of a Standard Based on Thermogravimetric Analysis of

Detergent Additives as an Interim CCD Control Measure. EPA requests

comment on whether a standard based on thermogravimetric analysis (TGA)

of detergent additives could be used as an interim measure to limit the

additive contribution to CCD. Such a standard would be based on the

premise that, to limit the additive contribution to CCD, a detergent

additive must decompose at temperatures encountered in the combustion

chamber. Any additive which does not decompose and burn in the

combustion chamber may provide material for the formation of CCD.

Thermogravimetric analysis is one method of determining the thermal

characteristics of materials, and might be useful in determining what

portion of detergent additive packages remain unburned and may

contribute to the formation of CCD.

One potential TGA-based standard would require that, as part of

detergent certification testing, a TGA analysis would be performed on

the detergent additive package. For a detergent to be certified, the

residue of the detergent package left at the specified temperature

would be required to not exceed a specified fraction by weight of the

original sample. Specifying a testing temperature is a critical element

in a potential TGA-based CCD control standard. Recent research

indicates that the surface temperature in the combustion chamber may be

the most important physical parameter in the formation of CCD.\9\ This

research indicates that, with high surface temperatures, CCD will reach

stabilized levels earlier and the total amount of deposits will be

lower. It further indicates that the critical surface temperature

beyond which no additional fuel-derived CCD form is 310 deg.C, and the

critical surface temperature beyond which no oil-derived deposits form

is approximately 60 deg.C higher. This research may be useful in

helping to determine the proper test temperature specification for a

TGA-based CCD control standard. EPA requests comment on an appropriate

temperature specification.

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\9\``A Physical Mechanism for Deposit Formation in a Combustion

Chamber'', Society of Automotive Engineers (SAE) Technical Paper

Series No. 941892.

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Comment is also requested on the allowable fraction of the additive

package which could remain as residue after the completion of the TGA

analysis. EPA believes that, for a TGA-based standard to provide a

meaningful measure of CCD control, the specification on the allowable

amount of residue would need to be set in the range of 2 percent of the

original sample. EPA requests comment on whether, alternately, it would

be more appropriate to place an absolute specification on the allowed

weight of detergent residue for a given quantity of additized gasoline,

and what an appropriate specification would be. Comment is also

requested on what procedural guidelines EPA should implement for the

TGA test.

The detergent additive package on which a TGA analysis was

performed would be required to contain the maximum concentration of the

detergent-active components covered under a registration. Use of these

components at higher concentrations to fulfill gasoline detergency

requirements would be prohibited. To enforce such a requirement, EPA

could require that samples of detergent additive be tested by the

additive manufacturer or submitted by the additive manufacturer for

analysis by EPA. A violation would occur if this sample failed to

satisfy the specified TGA-based limit. Alternately, a violation would

occur if, through fourier transform infrared spectroscopy (FTIR)

analysis, a sample was found to contain higher concentrations of

detergent-active components than those specified in the registration.

b. Use of Existing CCD Control Performance Data. One commenter

suggested that, as an interim measure, EPA require vehicle/engine CCD

control test data to be submitted by each detergent certifier without

detailing any requirements regarding the acceptability of the data. EPA

believes that such a requirement, while potentially encouraging

responsible consideration of CCD control by industry, would not provide

a meaningful measure of an additive's CCD control performance. EPA

believes that CCD control performance testing is too ill defined to

allow EPA to implement guidelines regarding its acceptability. The

Agency encourages public comment on this and other options that EPA

might adopt to control the potential adverse impacts of detergent

additive overuse.

D. Relationship to California Detergent Additive Program

Under EPA's proposed detergent certification requirements, a

detergent certified for use under the state of California's detergent

program (Title 13, section 2257 of the California Code of Regulations)

could be used to satisfy federal detergency requirements for gasoline

sold in California. The detergent additive certification requirements

currently implemented by the state of California include IVD/PFID

control requirements but do not include any unwashed gums or other CCD

control provisions. Therefore, if EPA were to implement an unwashed gum

standard or reporting requirement, a detergent certified by the

California Air Resources Board (CARB) would need to satisfy these

requirements in addition to complying with CARB's detergent

certification program in order to be eligible for use in complying with

federal detergency requirements in the state of California.

III. Other Issues for Additional Comment

A. Formulation of Certification Test Fuels

The discussion in this notice regarding the formulation of

certification test fuels pertains specifically to measures which EPA

might take to account for yet-to-be-identified nonoxygenate fuel

severity factors. Also discussed is the potential difference in the

deposit forming tendency of ethanol produced by different processes,

and measures that EPA might take to account for this variability. Other

issues related to test fuel definition will be addressed in the

detergent certification final rule.

1. Accounting for Unidentified Nonoxygenate Fuel Severity Factors

a. Approach Proposed in the NPRM. Under the proposed requirements,

certification testing for IVD/PFID control would normally be conducted

using a matrix of four test fuels, although testing in as few as two

fuels would be allowed under certain circumstances. Test fuels would be

required to meet or exceed minimum specifications regarding the levels

of the following four nonoxygenate fuel parameters which EPA believes

affect the deposit forming tendency of gasoline (referred to as fuel

severity factors): olefins, sulfur, aromatics, and T-90 distillation

point. To account for the deposit forming tendency of oxygenates, one

fuel would be required to contain 10 percent ethanol, and another would

be required to contain 15 percent MTBE. The NPRM included provisions

allowing other fuel parameters to be used to define certification test

fuels if their effect on IVD/PFID fuel severity could be demonstrated.

In the NPRM, EPA discussed concerns that specifications on these

fuel severity factors may not completely define a gasoline's deposit

forming severity. If this were the case, detergent certifiers might be

able to locate or specially blend certification test fuels that meet

the proposed compositional requirements but are still inappropriately

mild in their deposit forming tendency. To help account for unknown

factors in gasoline composition that may affect fuel severity, EPA

proposed that gasoline samples for certification testing must be drawn

from normal production gasoline stock (finished commercial gasoline)

taken from normally operating refinery and/or terminal facilities. In

addition, the multiple test fuels were to be drawn from separate

production/distribution facilities. This requirement would increase the

certainty that unknown severity factors will be represented by ensuring

that various refinery stocks are tested. It would also tend to limit

the opportunity to select test fuels from refineries that, for

unidentified reasons, tend to produce gasoline with a relatively low

deposit forming tendency.

b. Public Comment on the Proposal. Comments submitted by API and

CMA stated that requiring commercial fuels for testing would be

extremely burdensome and would have impractical consequences with

regard to the logistics and mechanics of obtaining non-additized fuel.

Amoco, API, CMA, Nalco, Texaco, and Ashland stated that EPA should

allow the use of refinery blend stocks that meet ASTM D4814

specifications to formulate certification fuels. It was also suggested

that the finished certification test fuels should meet ASTM D4814

specifications. One commenter stated that, to help alleviate concerns

regarding fuel blending, the identity of each blending component should

be documented regarding its source and properties.

AAMA stated that there might be characteristics that effect a

gasoline's deposit forming tendency which are not represented by

consideration of the five parameters proposed to define certification

test fuels. AAMA acknowledged that there are no data available to

determine which additional parameters would be appropriate to include

in the test fuel specifications. However, AAMA stated that

certification test fuels could be made more representative by requiring

that the major refinery streams be represented in the blending stocks

used to formulate these fuels. Such a practice would tend to help

ensure that yet-to-be-identified fuel severity factors are represented

in the certification test fuels. AAMA stated that requiring more than

one certification test fuel would allow for the inclusion of more

refinery streams in the formulation of certification test fuels,

thereby enhancing the representativeness of the testing.

Comments from API and CMA requested that EPA allow certification

testing on a single fuel, formulated from refinery blend stocks, that

contains each nonoxygenate fuel severity factor at its highest level in

the proposed test fuel matrix, plus 10 percent ethanol. These

commenters stated that the increase in gasoline deposit forming

tendency resulting from the addition of 10 percent ethanol is more than

enough to address concerns about the potential deposit forming tendency

of MTBE. Hence, testing on a second MTBE-containing fuel should not be

required. On the other hand, commenters from the automobile industry

stated that testing on both ethanol- and MTBE-containing fuels should

still be required to account for differences in their tendency to form

deposits.

c. Alternative Approaches that EPA Might Adopt. EPA is considering

several approaches, in addition to those proposed in the NPRM, to help

ensure the representativeness of the certification test fuels. Under

the first option, specifications on fuel parameters in addition to the

five that were proposed to be used to define certification test fuels

(olefins, sulfur, aromatics, T-90 distillation point, and oxygenate

content) would be added to better define the test fuels deposit forming

tendency. The NPRM discussed other fuel parameters that might have an

impact on a gasoline's tendency to form deposits. Several of these are

refinements on the nonoxygenate fuel parameters already considered.

The limited data available indicates that diolefins may affect a

gasoline's tendency to form deposits more significantly than do mono-

olefinic species. Certain species of sulfur, such as ditertiary butyl

disulfide, may also have more of an impact on a gasoline's deposit

forming severity than do other species of sulfur. In addition, limited

data suggests that heavier, polycyclic aromatic species may have a

greater impact on fuel severity than do other aromatic species. These

additional fuel parameters might be used in place of, or in addition

to, the less specific fuel parameters proposed in the NPRM (total

olefins, total sulfur, and total aromatics). Data were also discussed

in the NPRM suggesting that fuel nitrogen content might be useful in

helping to define the deposit forming tendency of certification test

fuels.

Nevertheless, the data available appears to be insufficient to

positively identify these fuel parameters as additional severity

factors. Also, since levels of such fuel parameters as diolefins,

ditertiary butyl disulfide, polycyclic aromatics, and fuel nitrogen are

not commonly measured or reported, it would be difficult to determine

what levels of these additional fuel parameters would be appropriate to

require in certification test fuels. As noted earlier, the proposed

test fuel specifications on the levels of sulfur, olefins, aromatics,

and T90 were based on national gasoline survey data. EPA requests

comments on what additional fuel parameters could be used to help

better define the severity of certification test fuels, and on the

levels of such fuel parameters that would be appropriate to require in

the test fuels to ensure adequate deposit control.

Given that it may not be feasible to use specifications on

additional fuel parameters to better define the severity certification

test fuels, EPA is considering several other alternatives to improve

their representativeness. One such approach would be to specify the

refinery blendstocks which must be used in the formulation of

certification test fuels. Due to their potential impact on the deposit

forming tendency of finished gasoline, EPA believes that specifications

on the minimum proportions of the following gasoline blendstocks to be

used in the formulation of certification test fuels may be useful in

helping to better define test fuel severity: full range fluid

catalytic-cracked (FCC) naphtha, full range reformate, full range

straight run naphtha, and light coker naphtha.

The relative proportions of these blendstocks required to be used

in the formulation of certification test fuels could be based on the

fraction at which they are used in blending finished gasoline in the

U.S. In keeping with the proposed certification test fuel

specifications, which require that each of the four nonoxygenate fuel

severity factors must be represented at levels greater than their

respective national average levels, it may be appropriate to require

that the subject blendstocks be represented in the certification test

fuels at proportions that exceed their average representation in

finished U.S. gasoline. Based on this approach, appropriate

specifications on the minimum percentage of the subject refinery

blendstocks which must be used in formulating the certification test

fuels are likely to fall within the following ranges: 25 to 40 percent

full range FCC naphtha, 25 to 40 percent full range reformate, 1 to 3

percent full range straight run naphtha, and 1 to 3 percent light coker

naphtha.\10\ These specifications would account for approximately 50 to

85 percent of the gasoline blendstocks used in formulating

certification test fuels. The remaining blending components used in

formulating the test fuels could be drawn from any type of refinery

blendstock.

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\10\For a review of the quantities of manufactured gasoline

blendstocks blended into U.S. gasoline during the period of April 1

through September 30, 1989, see the National Petroleum Refiners

Association Survey of U.S. Refining Industry Capacity to Produce

Reformulated Gasolines, part A, January 1991.

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EPA requests comment on the usefulness of this approach in

accounting for yet-to-be-identified fuel severity factors and in

preventing the use of certification test fuels with inappropriately

mild deposit forming severity. EPA specifically requests comment on

which refinery blend stocks should be included and on the proportions

at which they should be represented in the test fuels. EPA also

requests comment on the number of test fuels which would be needed to

adequately represent all the relevant refinery blend stocks given the

need to meet EPA's proposed fuel compositional specifications

(regarding minimum required levels of olefins, sulfur, aromatics, T-90,

and oxygenates). EPA believes that a single test fuel may not be

adequate for this purpose. In addition, the Agency requests comment on

the extent to which previous commenters concerns regarding potential

logistical problems associated with EPA's proposal to require testing

of finished commercial fuels also apply to the approach of formulating

test fuels from specified proportions of particular refinery blend

stocks.

Another approach EPA is considering would involve raising the

levels of the four nonoxygenate fuel parameters required in the

certification test fuels. This approach may be useful in helping to

limit the variability in fuel severity for a given fuel specification,

because the extent of this variability may tend to decrease as levels

of these fuel parameters increase. EPA is considering requiring that

the 65th percentile levels of these four nonoxygenate fuel parameters

must be present in the certification test fuels after the addition of

oxygenates, rather than before their addition as was proposed. This

approach is being considered due to public comment on the NPRM which

indicated that allowing the levels of these fuel parameters to be

diluted by the addition of oxygenate may inappropriately reduce test

fuel severity. If EPA were to take such an approach, the resulting

increase in fuel severity may tend to reduce concerns over the

variability in fuel severity due to the effect of yet-to-be identified

fuel parameters. EPA requests comment on the extent to which

variability in test fuel severity would continue to be a concern if

such an approach were adopted.

EPA also requests comment on whether it would be appropriate to

increase the required levels of the nonoxygenate fuel parameters still

further to limit the variability. To this end, EPA is considering

requiring that each of the nonoxygenate fuel parameters must be

represented in the certification test fuels at their respective 70th

percentile levels after the addition of oxygenate. Such comment should

also address the potential that such an upward adjustment in test fuel

severity may cause higher concentrations of detergent additive to be

used, with an associated heightening of concerns regarding the additive

contribution to the formation of CCD.

Another approach EPA is considering would require that the deposit

forming tendency of test fuels be demonstrated through testing of the

non-additized fuels prior to their use for certification testing

purposes. Under this approach, each test fuel would be evaluated for

its tendency to form intake valve deposits using the BMW 318i test

procedure (as adopted by EPA for certification testing). The cost of

implementing such a requirement would naturally increase with the

number of test fuels required, and its adoption would be most

economical if only a single test fuel formulation were required. For a

fuel to be acceptable for use in certification testing, a specified

deposit weight would need to be accumulated during pre-certification

testing of the fuel in an unadditized state. EPA is considering several

alternative test fuel evaluation criteria. Under the first alternative,

at least 150-250 mg of intake valve deposits (on average) would be

required to be accumulated over the course of 10,000 test miles for a

test fuel to be acceptable. Under the second alternative, at least 80-

120 mg of IVD would be required to be accumulated over the course of

5,000 test miles. Specific comment is also sought on point values

within the two mg ranges presented above.

EPA requests comment on whether this approach is a necessary and

useful measure to ensure the representativeness of certification test

fuels. Comment is requested on whether it would be useful to require

that fuels meet compositional specifications if EPA were to require

that they be tested to demonstrate adequate deposit forming severity

prior to use for certification purposes. Specific comment is requested

on the level of IVD that should be required to be generated for a test

fuel to be acceptable as having an adequately severe deposit forming

tendency. EPA also requests comment on whether it is necessary to

require demonstration of a test fuel's tendency to form fuel injector

deposits (PFID) and the appropriate test/standard which might be used

to accomplish this purpose. One option under consideration is use of

the Chrysler 2.2L vehicle in the ASTM test with the fuel required to

generate a flow restriction in the range of 10-20 percent. Specific

comment is requested on this option including a point in the range and

also on whether a bench rig test may be sufficient to screen a test

fuel for its tendency to form PFID. Comment is also requested on other

measures which may be implemented to ensure the representativeness of

certification test fuels.

2. Accounting for Potential Variability in the Deposit Forming Severity

of Ethanol

EPA proposed that the ethanol used in formulating certification

test fuels must be of fuel-grade quality. Specially processed ethanol

would not be acceptable for use in formulating certification test

fuels. This requirement was proposed to account for the deposit forming

tendency of other substances commonly found in fuel-grade ethanol. EPA

now believes that depending on the processing method used to produce

fuel-grade ethanol, various levels and types of impurities may be

present. These varying levels of these impurities, such as fatty acids,

might potentially effect the deposit forming severity of fuel-grade

ethanol to different degrees. If this were the case, certification

testing could be conducted using fuels blended with fuel-grade ethanol

that has an inappropriately low tendency to increase gasoline forming

tendency.

EPA requests comment on the extent to which this is a concern and

on potential approaches that EPA might take to ensure that the ethanol

used during certification testing is representative of in-use ethanol

blending stock in its tendency to from deposits. One approach would be

to require that ethanol used for certification testing purposes must

contain a minimum level of impurities. Specifications might also be

necessary on the type of impurities which must be present. The maximum

allowed levels of impurities specified in commercial standards for

fuel-grade ethanol might be useful in determining the levels of

impurities that must be present in ethanol used for certification

testing. Potable and chemical grade ethanol as well as fuel grade

ethanol which receives additional processing not common to all fuel

grade ethanol could not be used in testing. EPA also requests comment

on the extent to which the concerns discussed above may also apply to

MTBE used in certification testing. EPA also asks for comment on

whether the restrictions discussed above for ethanol should also be

applied to MTBE.

B. ASTM IVD and PFID Control Test Procedures

In the NPRM, EPA proposed test procedures to evaluate IVD and PFID

control that were largely based on draft procedures under evaluation by

the American Society for Testing and Materials (ASTM) at the time of

the proposal. EPA also proposed that the ASTM test procedures might be

adopted in the detergent certification final rule if they were

finalized by ASTM in time, and there were no changes that would require

further public notice and comment.\11\ These test procedures have

recently been finalized by ASTM and EPA anticipates their adoption

under the detergent certification final rule.\12\ EPA requests comment

this approach. EPA proposed an alternate IVD control standard at a

5,000 mile test length, in addition to the traditional 10,000 mile

standard. Comment is requested on what addition to the ASTM IVD control

procedure would be necessary to allow the use of a 5,000 mile test

length as well as the 10,000 mile test length specified by ASTM.

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\11\Drafts of the ASTM IVD and PFID test procedures were placed

in the public docket for review.

\12\The ASTM procedures are designated as follows: ASTM test

method D 5500, ``Standard Test Method for Evaluation of Unleaded

Automotive Spark-Ignition Engine Fuel for Intake Valve Deposit

Formation'', and ASTM test method D 5598, ``Standard Test Method for

Evaluating Unleaded Automotive Spark-Ignition Engine Fuel for

Electronic Port Fuel Injector Fouling''.

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C. Applicability of Gasoline Detergency Requirements

The gasoline detergency requirements implemented by the interim

detergent registration rule apply to all gasoline, leaded and unleaded,

highway and off-road, including both reformulated and conventional

gasolines, oxygenated gasoline, and the gasoline component of M85 and

E85, as well as marine fuel and gasoline for military purposes. (M85 is

a mixture of 85% methanol and 15% gasoline. E85 is a mixture of 85%

ethanol and 15% gasoline.) Gasoline service accumulation fuel is also

required to comply with gasoline detergency requirements, as is the

gasoline component of alcohol blend service accumulation fuel. As noted

in the detergent registration final rule, the following types of

gasoline are exempted from compliance: aviation fuel, racing fuel,

emissions certification fuel, and gasoline used for research and

developmental purposes. Gasoline detergency requirements apply to all

gasoline other than those types for which an exemption was specifically

prescribed.

As an example, although not specifically mentioned in the

regulation, since it is to be used in highway motor vehicles factory

fill fuel must comply with gasoline detergency requirements.\13\

Factory fill fuels must comply with these requirements despite the

exemption from general fuel registration requirements noted for these

fuels in 40 CFR 79.4(a)(3).

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\13\Factory fill fuels must comply with these requirements

despite the exemption from general fuel registration requirements

noted for these fuels in 40 CFR 79.4(a)(3).

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An automobile manufacturer recently suggested to EPA that certain

detergent additives used in the gasoline portion of E85 may contribute

to the formation of deposits in vehicle fuel pumps in E85 vehicles.\14\

EPA requests comment on the potential incompatibility of certain

detergent additives for use in the gasoline portion of E85, and on the

regulatory measures which EPA could take to address such a problem if

it exists. Comment is also requested on the extent to which such

concerns might also apply to M85 fuel.

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\14\Memorandum entitled: ``Phone Call with Gerald Barnes of

General Motors Regarding the Potential Incompatibility of Certain

Detergent Additives for use in the Gasoline Portion of E85 fuel.'',

Docket Item IV-E-34

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D. Aftermarket Detergent Additives

The proposed detergent certification program did not cover the use

of aftermarket detergent additives.\15\ EPA requests comment on whether

any requirements regarding the deposit control efficiency of

aftermarket additives should be implemented, and the authority under

which EPA could act to implement such requirements. Specifically, EPA

requests comment on what requirements might be necessary on aftermarket

additives to limit their potential contribution to the formation of

CCD. This is of particular concern since EPA believes that the

manufacturers of such aftermarket additives advise their use at very

high concentrations to remedy PFID/IVD related problems. As discussed

earlier, potential interim CCD control options involve limiting the

concentrations used of detergents which have a tendency to form CCD.

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\15\Aftermarket detergent additives are marketed directly to

gasoline consumers for addition directly into the vehicle fuel tank.

---------------------------------------------------------------------------

E. Detergent Additives Certified for Use in California Phase-2

Reformulated Gasoline

The interim detergent registration rule specified that data used to

support the certification of detergent additives under California's

detergent additive program, specifically for use in California Phase-2

Reformulated Gasoline, will be acceptable for use in demonstrating the

performance of detergents used to comply with Federal detergent

gasoline requirements only for gasoline sold within the state of

California. During a workshop on the interim requirements for deposit

control additives, held by the American Petroleum Institute (API) on

October 26, 1994, commenters from the audience suggested that EPA

should allow California Phase-2 reformulated gasoline that is additized

with detergents certified under California's detergent additive program

to be sold outside of California. EPA agrees that this approach is in

keeping with the goals of this program. The addition of such a

provision would also allow improved flexibility in the gasoline

distribution system.

Therefore, EPA proposes to amend the provisions of the interim

detergent rule to provide that gasoline additized within the state of

California in accordance with the requirements of the California Air

Resource Board's (CARB's) detergent rule may also be sold outside of

the state of California. Specifically, EPA proposes to amend section

80.141(e)(1) of the regulatory text to state that, under the interim

program, CARB detergent certification data specific to California

phase-2 reformulated gasoline will be accepted as adequate support of

detergent effectiveness for detergent gasoline that is blended within

the state of California in accordance with CARB's detergent program.

F. Allowed Variation in the Concentration of Detergent-Active

Components Within a Single Registration for a Detergent Additive

Package

During the workshop on the interim requirements for deposit control

additives held by API, commenters from the audience requested

clarification of the allowed variation in the concentration of

detergent-active components in a detergent additive package under a

single additive registration. They stated that it is not possible to

comply with the requirements of section 80.141(c)(2), which state that

no variation is allowed in the concentration of any of the detergent-

active components under a single variation, given variability in

manufacturing process. They further stated that upward variation in the

concentration of these components should be allowed, since such

variation would not compromise the additive's deposit control

efficiency. Indeed, as suggested by these commenters, EPA intended the

language of section 80.141(c)(2) to prevent downward variation in the

concentrations of the detergent-active components from the minimum

concentrations reported in the subject additive registration. It was

not intended to prevent an upward variation in the concentration of

these components. Therefore, to clarify this provision, EPA proposes to

amend section 80.141(c)(2) to state that upward variation in the

concentration of detergent active components would be permitted,

provided that such variation is specified in the registration, and that

such variability does not change the minimum recommended concentration

reported to be necessary to control deposits.

G. Enforcement Issues

EPA has several enforcement issues for which comments are requested

prior to the issuance of the certification final rule. EPA believes

these issues are integral to successful enforcement of the detergent

program, and will be addressing these issues in the certification final

rule.

1. Meters

a. Required Use of Meters on Automated Additization Systems.

In the NPRM, the proposed mass balance (now volumetric additive

reconciliation, or ``VAR'') formulas provided for three different

additization systems: hand blending, meters on every injector, and a

metering system that did not have meters on every injector. EPA

requested comments on whether the certification rule should require,

for the purpose of measurement accuracy, that automated additization

equipment be equipped with meters on every injector.

EPA received no comments specifically addressing this issue.

However, API commented that the final automated VAR formulas should be

flexible enough to permit the use of presently existing automated

additization equipment, which includes meters on every injector,

metered systems without meters on every injector, and automated systems

without any meters that measure detergent use through tank inventory

gauging.

The VAR formula in the interim program final rule does not require

automated detergent blenders to have metered measurement systems, in

deference to lead time concerns. However, as was proposed in the NPRM,

EPA does intend to require some form of metered measurements for

automated detergent blenders in the certification program final rule.

EPA is still interested in receiving comments about the value of

requiring systems with meters on every injector, as opposed to

permitting the use of metered systems that measure the flow from many

injectors on one meter.

A metered measurement system will be required in the certification

program final rule because meters are unquestionably a more accurate

measurement system than tank inventory gauging. Meters measure the

actual flow of product going through them, while inventory gauges

merely determine drop in tank volume. As API commented in its analysis

of automated additization system errors, inventory measurement systems

are subject to error both in measuring inventory as well as in

measuring additions to inventory. API's own member survey, submitted to

EPA as comment, suggested that metered systems would need a smaller

accuracy tolerance range than inventory systems, i.e., an 8 to 10

percent tolerance based on metered system errors, as opposed to the

greater 10 to 15 percent tolerance range based on inventory system

errors. (Parenthetically, an enforcement tolerance was not provided in

the interim program final rule and is not anticipated in the

certification program final rule. This issue was addressed at length in

the preamble to the interim program final rule.)

The final detergent certification program rule, expected to be

effective in mid-1996, will not have the lead time issues associated

with implementation of the interim program. EPA therefore reconfirms

its proposal that, under the final certification program, all automated

detergent blenders using the automated formula be required to have

metered measurements. Furthermore, to assure accuracy of the VAR

measurements, EPA proposes that all metered systems must include meters

on every injector. This more stringent proposal recognizes that not all

metered systems can accurately establish whether gasoline is being

appropriately additized. If the system merely has a master meter which

measures, in the aggregate, the flow of detergent from the tank into a

multitude of injectors, it is not possible to determine whether any

particular injector is operating properly and dispensing the proper

amount of detergent. To ensure that each injector is dispensing the

appropriate detergent concentration, a meter would have to be installed

on each injector.

Obviously, EPA wants to fulfill its statutory mandate of ensuring

the proper additization of gasoline to prevent deposits, and believes

it is necessary to require all automated systems to be equipped with

meters on every injector. However, the Agency is also concerned about

the costs of such a requirement, and is therefore very interested in

receiving comments about the number of automated blenders that would

need to upgrade under such a requirement, the cost that would accrue to

such blenders, as well as the aggregate cost. The Agency would then be

interested in comparing these costs with the value received in

additional additization accuracy expected to result from this

requirement.

b. Precision of Metered Measurements. The NPRM proposed that VAR

detergent measurements for automated blenders be determined and

recorded to one tenth of a gallon. API commented that detergent volume

measurement should only be required to be recorded at the gallon level,

since scaling back the determination to precision of a gallon would be

necessary to accommodate all present additization systems. In deference

to the concern that some parties would be unable to upgrade to systems

with precision to at least one tenth of a gallon in time for the

January 1, l995 implementation date of the interim program rule, the

interim program requires VAR detergent measurements to be recorded only

to the nearest gallon.

EPA is now proposing that, under the certification program final

rule, the VAR detergent measurements for automated blenders must be

recorded to a precision of at least one tenth of a gallon. This

provision is consistent with the proposal that all automated blenders

using the automated VAR formula must be equipped with metered detergent

measurement equipment. It is EPA's understanding that metered equipment

is easily able to measure to the one tenth of a gallon precision

standard, and it should not be difficult for regulated parties to meet

this higher level of precision once the provisions of the certification

program go into effect. Comments are requested about the measurement

capabilities of metered measurement equipment and about the

reasonableness of requiring recording accuracy to one tenth of a

gallon.

2. The Use of a Per-Gallon Minimum Detergent Requirement within VAR

Compliance Periods for Automated Detergent Blenders

In the NPRM, EPA proposed that all detergent blenders conduct

regular product reconciliations to determine the accuracy of their

additizations. Hand blenders were proposed to perform this

reconciliation on a per-batch basis, whereas automated blenders, not

having the uniform capability to easily determine per-batch usage, were

proposed to perform the reconciliations on a weekly basis.\16\ The

detergent reconciliation proposed for automated blenders was, in

effect, an averaging procedure, permitting automated blenders to

calculate the accuracy of their additization throughout the compliance

period on an averaged basis.

---------------------------------------------------------------------------

\16\In fact, pursuant to comments, the interim program requires

only a monthly reconciliation period for automated blenders.

---------------------------------------------------------------------------

To limit the ability to average detergent usage, EPA also proposed

in the NPRM that any intentional alteration of the detergent

concentration within the compliance period would terminate the period

and necessitate the start of a new period. Under this proposal,

intentional compensation for under-additization discovered in the

period would not be permitted. However, in its comments, API expressed

concern that, without a significant enforcement tolerance to determine

compliance with the VAR standard over the entire period, automated

detergent blenders in some circumstances would be required to make

concentration adjustments in order to stay in compliance. As explained

in detail in the interim program final rule, EPA did not believe it was

appropriate to create a VAR standard enforcement tolerance, but did

decide to permit limited intentional compensation within the compliance

period for discovered under-additizations. The permissible adjustment

was limited to 10 percent above the concentration initially used in the

period. The purpose of this limitation was to prevent blenders from

attempting to compensate for substantial under-additizations (and thus

avoid liability for such under-additizations) by means of intentionally

over-additizing, to a significant degree, for the rest of the period.

However, the Agency still has concerns that permitting averaging

over the automated blender VAR compliance period will tolerate

unacceptable amounts of per-gallon under-additization of gasoline.

Depending on the amount of additized gasoline measured in the

compliance period, it is clear that even the 10 percent adjustment

limitation could permit some quantity of gasoline being non-additized

or significantly under-additized. Even if serious under-additization

occurred early in the period, the averaged compliance standard might

still be attained by the blender through the permissible upward

adjustment of the detergent concentration rate for the rest of the

period.

Naturally, EPA would like to ensure that all gasoline is additized

at an effective detergent concentration rate, as established during

certification testing. The VAR compliance procedures included in the

interim program go a considerable way toward accomplishing this goal,

but only on an average for the compliance period. Individual loads of

gasoline may still be severely out of specification. Consequently, for

the final certification program rule, EPA is proposing that, within the

monthly compliance period for automated blenders, each load of the

product must be additized at a rate that is at least 90 percent of the

certified detergent treat rate. This 90 percent figure would allow for

some lapse in equipment efficiency while providing assurance that each

load in the averaging period will approximate the certification

standard. The reasonableness of the proposed 90 percent minimum

requirement is supported by on an API member survey which was submitted

as a comment to EPA. This survey indicated that many blenders (73 per

cent of proprietary systems, and 37 percent of non-proprietary systems)

can apparently attain a monthly blending accuracy to within 10 per cent

of the goal.

The minimum per-gallon requirement within the averaged VAR

compliance standard would not only provide greater assurance of across-

the-period accurate additization, but would also provide EPA with a

useful enforcement tool. With this per-gallon minimum, EPA would be

able to sample and test additized gasoline for detergent program

compliance at the facilities of any regulated party. Under the interim

program, on the contrary, the testing of additized product may reveal

complete non-additization without necessarily establishing a violation,

since there is no minimum per-gallon requirement under the interim

period's VAR procedures. Although extensive sampling and testing of

additized product is not presently contemplated, the ability to conduct

such testing on a case-specific basis and to establish violations based

on such testing would be very useful.

EPA is requesting comments on the proposed per-gallon minimum

requirement within the VAR compliance procedures. The Agency is

particularly interested in learning whether the 90 percent minimum

requirement is considered attainable, what problems would be associated

with this minimum requirement, what records would be useful in

monitoring compliance with the requirement, and what the costs would be

in attaining compliance with a minimum standard. Comment is also

requested on an alternate per-gallon minimum requirement, with

rationale to support its adoption instead of a 90 percent minimum

requirement. If commenters believe the per-gallon minimum concept is

not appropriate, EPA requests suggestions for alternative means to

assure greater additization accuracy throughout the VAR compliance

period. One such alternative option being contemplated by the Agency is

the previously proposed weekly compliance period, which would obviously

permit less extensive averaging than the longer, monthly period.

3. Presumptive Liability for VAR Violations

Under the interim program final rule, only detergent blenders will

be held liable for VAR violations. However, EPA stated in the preamble

to interim program rule that this issue may be revisited in the

detergent certification final rule. Although some commenters asserted

that detergent blenders should be the only parties liable for VAR

violations, EPA believes that parties other than, or in addition to

detergent blenders, could cause VAR violations. Therefore, limiting

liability for VAR violations to detergent blenders may allow culpable

parties to evade liability for VAR violations that they have caused.

For example, a party may cause VAR violations by providing

inaccurate or incomplete blending instructions to detergent blenders,

or by conspiring with detergent blenders to sell under-additized

gasoline that violates VAR requirements. The latter scenario could come

about if a retailer attempted to save money by intentionally purchasing

cheaper, unadditized or under-additized gasoline from a terminal which

was intentionally violating VAR requirements to produce such gasoline.

In this scenario, the collusion would occur because the retailer would

benefit from the lower cost of its purchased gasoline, and the terminal

would benefit from the sale of the misadditized product to the

retailer.

Further, the newly proposed per-gallon minimum requirement within

the VAR procedures would make it possible for EPA to effectively

discover VAR per-gallon minimum violations downstream, at retail

outlets or at other regulated parties receiving product from the

detergent blenders. When such violations are found, EPA needs the

ability to hold these parties liable for such VAR violations. As shown

in the preceding paragraph, it clearly could be in the financial

interest of these parties to cause VAR violations by colluding with

detergent blenders to sell VAR violating, less expensive gasoline.

EPA believes that parties who cause VAR violations should not

escape liability for those violations. Therefore, EPA is considering as

an option under the detergent certification final rule, that all

parties in the misadditized product's distribution system, including

detergent blenders but excepting upstream carriers, will be

presumptively liable for such VAR violations. As is typically the case,

carriers upstream to where a violation is found will be liable for such

violations if EPA can establish that they caused the violation.

The rationale for imposing a presumptive liability scheme for VAR

violations would be the same as that which supports presumptive

liability for other violations in the detergent program, and for

violations of other EPA fuels programs such as reformulated gasoline,

gasoline volatility, and lead contamination. Typically, many parties

handle and control gasoline, detergent and detergent-additized post-

refinery component, which are, often times, fungible products. Under

these circumstances, it will be difficult for EPA to determine who, in

addition to the detergent blender, might have caused the VAR

violations. When multiple parties potentially may have caused a

violation, the Agency needs a presumptive liability scheme to

effectively enforce its regulatory program.

All presumptively liable parties would have the right to establish

an affirmative defence to such liability. EPA expects that the vast

majority of VAR violations will be caused by detergent blenders, and in

these cases, the blenders will be the only parties liable.

EPA requests comments on the issue of presumptive liability for VAR

violations, including comments regarding EPA's legal authority to

impose such liability. Parties disagreeing with EPA's proposed approach

are urged to submit alternative options to address the problem of

multiple party causation of VAR violations. One alternative approach

that EPA is considering, and is requesting comment on, is the

imposition of an affirmative duty (with attendant penalties) on

upstream parties transferring title to detergent or custody to those

who will physically do the blending, to transfer accurate written

blending instructions for use of that detergent. In addition, a new

liability section would be created which would hold any regulated party

liable for a VAR violation if EPA could establish that the party caused

the violation.

4. Right of Entry to Inspect the Premises of Regulated Parties in the

Detergent Distribution System

Current regulations permit EPA to enter the premises of gasoline

refiners, retailers, wholesale purchaser-consumers, distributors, and

importers, and to make inspections, take samples, and conduct tests at

such facilities to determine compliance with EPA requirements. See 40

C.F.R. 80.4. EPA is today proposing to amend this provision to include

manufacturers, distributors, and carriers of detergent additives.

To investigate possible violations of detergent specifications

promulgated under Sections 211(l) and 211(c), and to ensure compliance

with those specifications, it is necessary for EPA to have the ability

to collect samples of detergent additives at the facilities of the

detergent manufacturer, distributor, and carrier. Section 211(l)

directs EPA to establish, by regulation, specifications for detergent

additives that must be used to prevent the accumulation of engine or

fuel system deposits. EPA must be able to sample the detergent additive

before it is blended into gasoline to ensure that manufacturers produce

detergents that comply with EPA regulations, and to ensure that

distributors and carriers of detergents do not take actions that alter

detergents in such a way that the requirements are not met. Further,

this approach is consistent with the currently existing provision in

Part 80 under which EPA may enter the facilities of gasoline refiners

and other parties, and make inspections, take samples, and conduct

tests at such facilities to determine compliance with the requirements

of that part.

Therefore, under EPA's broad authority under Section 301(a) to

promulgate such regulations as are necessary to carry out the Agency's

functions under the Act, and EPA's authority under Sections 114,

211(c), and 211(l), EPA is proposing to amend the currently existing

right of entry provision in 40 C.F.R. 80.4 to include detergent

manufacturers, distributors, and carriers. Also, see Dow Chemical Co.

v. United States, 476 U.S. 227 (1986), recognizing EPA's broad

authority to use reasonable means to carry out its investigatory

function under the Act, including but not limited to Section 114. EPA

invites comment on this proposed amendment.

5. The Use of Multiple Detergent Concentrations by Automated Detergent

Blenders

Under the proposed regulatory approach published in the NPRM,

automated detergent blenders were not permitted to include several

detergent concentrations in one VAR compliance record. Any change in

concentration under the NPRM would have necessitated the start of a new

VAR period. The purpose of this limitation was to prevent the attempt

by blenders to compensate for significant under-additization within a

compliance period by changing the rate of additization in the rest of

the period.

The Agency received a comment protesting this prohibition against

the use of several detergent set rates in one VAR record. The commenter

argued that this restriction would penalize blenders with sophisticated

equipment that could automatically change set rates depending on the

product being additized. According to this commenter, such a blender

would be required to create a new VAR record every time his equipment

automatically switched concentration rates to accommodate different

grades of product being additized.

EPA does not intend to discourage the use of sophisticated

additization equipment by detergent blenders. Therefore, under the

interim program EPA did not prohibit the use of several set rates on a

single VAR record. However, blenders are required to meet the following

conditions under the interim program to ensure additization accuracy:

no concentration set rate can be set below the detergent's lowest

additive concentration (LAC); each initial set rate used in the period

must be recorded on the VAR record, along with the product to be

additized with each rate; no adjustments to the initially set rates can

be made in the period above 10 percent of the initial rate; the blender

must maintain records of all adjustments to the set rates.

These requirements protect additization accuracy, while at the same

time, provide industry with the flexibility to use sophisticated

additization equipment capable of automatically varying set rates. The

Agency continues to believe that these VAR requirements are useful.

However, further restrictions are necessary to ensure additization

accuracy under the detergent certification final rule.

Under the interim program, automated blenders can measure on a

single VAR record product being additized by the same detergent under

different set rates, as long as they meet the conditions stated above.

Since VAR compliance under the interim program is an averaged

compliance, there is no way to determine under this procedure if the

product being additized at the lower rate is actually meeting its LAC

requirements, because the product being additized at the higher rates

would conceal any failure of the lower product to meet the averaged

standard. This procedure of multi-rate averaging is thus not conducive

to assuring the additization of all product.

Consequently, EPA is proposing that, under the detergent

certification final rule, automated blenders may continue to blend

their detergent at multiple rates in one VAR period, but product being

blended at each set rate must have its own VAR record. This would

ensure that product additized at each rate meets the LAC standard.

Further, the Agency is also proposing that a blender choosing to use

different set rates within a single VAR period must have equipment that

can accurately measure detergent use at each set rate, (e.g. meters

which can switch to measuring different rates, meters on individual

injectors measuring different rates, or other effective systems). This

latter requirement will ensure that the accuracy of each set rate's

additization can be effectively measured, not merely estimated or

assumed.

Comments are requested about these proposed changes to automated

blender VAR requirements. Specifically requested is information about

the cost associated with implementation of these changes, such as the

number of blenders they would impact, the number of blenders that would

be forced to upgrade their equipment to accommodate these changes, and

the cost of such upgrades. If commenters are opposed to the

implementation of these changes, they are urged to submit alternative

plans to address the problem of ensuring proper additization of product

additized at lower concentrations when multiple concentrations are

being measured.

6. Regulation of Imported Additized Gasoline

Under the NPRM, importers of gasoline are regulated parties,

subject to the requirements of the detergent rule. They are thus

subject to product transfer document requirements and the prohibitions

against the transfer and sale of nonconforming product. They are

permitted to import either additized or nonadditized product. If they

additize the gasoline they import, they are considered detergent

blenders, and are subject to VAR requirements for the gasoline. If they

import additized gasoline but are not detergent blenders, they are not

required to create and maintain VAR records establishing VAR

compliance. However, if the product they import is sampled and shown to

be under- additized, the importer would be presumptively liable for the

violation. As a practical matter, it would be extremely difficult for

the importer to effectively meet its affirmative defence requirements,

unless it would provide EPA with the VAR records documenting proper

additization of the product.

The Agency believes the control over imported gasoline needs to be

strengthened in regard to gasoline which is additized prior to

importation. As was extensively discussed in the NPRM, enforcement of

the detergent regulation will primarily be based on record review,

since sampling and testing of additized gasoline for compliance will be

difficult. Agency review of VAR records to determine accurate

additization is thus critical to the success of the program. It is just

as important for EPA to be able to review VAR records for imported

gasoline which is additized, as it is to review those records for

domestic product, given the sampling and testing limitation. Under the

interim program, however, Agency review of VAR records for imported

additized gasoline will be limited to those situations in which

violations have already been discovered through testing or otherwise.

This means that, in regard to imported gasoline, the Agency is deprived

of its prime measures to determine detergent program violations.

To correct this deficiency, EPA is proposing that the detergent

certification final rule will amend the definition of detergent blender

to include importers of additized gasoline within the definition. If

importers choose to import additized product, they must be held

accountable for its additization accuracy as detergent blenders. If

not, those selling domestically additized gasoline will be at a

disadvantage to importers, since VAR records establishing violations

will not be generally available for EPA review. Including importers of

additized product within the definition of detergent blender will make

the importers responsible for the creation and maintenance of the VAR

records verifying additization accuracy, as well as with compliance

with the other VAR requirements that apply to domestically additized

product. EPA requests comments about the proposed amendment of the

definition of detergent blender.

IV. Public Participation

EPA has encouraged full participation of the regulated industry and

other interested parties in the development of the rule to implement

the statutory requirements and continues to do so. A public workshop

was held on February 13, 1992 to initiate open discussion of the

relevant issues and EPA met with numerous industry representatives

separately to obtain their input.

The Notice of Proposed Rulemaking (NPRM) was published on December

6, 1993 (58 FR 64213) and a public hearing was held in Ann Arbor,

Michigan on January 11, 1994. Comments on the NPRM were accepted until

March 11, 1994. EPA received 31 written comments on the NPRM before the

close of the initial comment period and has received additional

comments since that time particularly with respect to the issues

discussed in this notice. EPA encourages additional comment on the

issues discussed in this notice through the close of the current

comment period. (For the date on which the comment period closes see

the Dates section in this notice.) EPA does not intend to hold an

additional public hearing to discuss the issues raised in this notice.

V. Electronic Copies of Rulemaking Documents

Electronic copies of this notice, and other documents associated

with the detergent certification rule are available on the Office of

Air Quality Planning and Standards (OAQPS) Technology Transfer Network

Bulletin Board System (TTNBBS). Instructions for accessing TTNBBS and

downloading the relevant files are described below.

TTNBBS can be accessed using a dial-in telephone line (919- 541-

5742) and a 1200, 2400, or 9600 bps modem (equipment up to 14.4 Kbps

can be accommodated). The parity of the modem should be set to N or

none, the data bits to 8, and the stop bits to 1. When first signing on

to the bulletin board, the user will be required to answer some basic

informational questions to register into the system. After registering,

proceed through the following options from a series of menus:

(T) GATEWAY TO TTN TECHNICAL AREAS (Bulletin Board)

(M) OMS

(K) Rulemaking and Reporting

(3) Fuels

(4) Detergent Additives

At this point, the system will list all available files in the

chosen category in chronological order with brief descriptions. The

following five ``.ZIP'' files are currently available:

``DCA__PRE.ZIP'' (Preamble from the Notice of Proposed Rulemaking)

``DCA__IFP.ZIP'' (Preamble to the final rule on the Interim

Requirements for Deposit Control Additives)

``DCA__IFR.ZIP'' (Regulatory text for the final rule on the Interim

Requirements for Deposit Control Additives)

``DCA__RIA.ZIP'' (Regulatory Impact Analysis)

``DCA__RCN.ZIP'' (Notice to Reopen the Comment Period)

File information can be obtained from the ``READ.ME'' file. Choose

from the following options when prompted:

ownload, rotocol, xamine, ew, ist, elp or to

exit.

To download a file, e.g., filename.ZIP, the user needs to

choose a file transfer protocol appropriate for the user's computer

from the options listed on the terminal. The user's computer is then

ready to receive the file by invoking the user's resident file transfer

software. Programs and instructions for de-archiving compressed files

can be found under ystems Utilities from the top menu, under

rchivers/de-archivers. Please note that due to differences between

the software used to develop the document and the software into which

the document may be downloaded, changes in format, page length, etc.

may occur.

TTNBBS is available 24 hours a day, 7 days a week except Monday

morning from 8-12 EST, when the system is down for maintenance and

backup. For help in accessing the system, call the systems operator at

919-541-5384 in Research Triangle Park, North Carolina, during normal

business hours EST.

V. Statutory Authority

The statutory authority for the regulation of gasoline detergent

additives is granted to EPA by sections 211 (c) and (l) of the Clean

Air Act, as amended, 42 U.S.C. 7414, 7545 (c) and (k), and 7601.

List of Subjects in 40 CFR Part 80

Environmental protection.

Fuel additives, Gasoline detergent additives, Gasoline motor

vehicle pollution, Penalties, Reporting and recordkeeping requirements.

Dated: December 19, 1994.

Richard D. Wilson,

Acting Assistant Administrator for Air and Radiation.

[FR Doc. 94-31815 Filed 12-27-94; 8:45 am]

BILLING CODE 6560-50-P

This is a copy of a public record, reproduced as it was published. It is not legal advice, and it may not be the version a court would rely on. Check the official source before you cite it.

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